Perchloric acid is a corrosive liquid that is colorless, odorless, and oily in nature. It is a strong acid that can be highly oxidizing and has the potential to react violently with certain materials, posing a fire and explosion hazard.
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Potassium Hydrogen Phthalate Extrapure AR, 99.9% is slightly acidic, and it is often used as a primary standard for acid–base titrations because it is solid and air-stable, making it easy to weigh accurately.
The purpose of adding sodium thiosulfate is to remove the excess iodine from the reaction mixture. This is important because iodine is a strong oxidizing agent and can cause side reactions with the organic compounds in the mixture.
Methyl orange is a popular pH indicator that is used in the titration. The colour of the solution turns red when methyl orange is used as an indicator of acid. When methyl orange is mixed with a base, the result is yellow, or the colour changes to yellow. As a pH symbol, methyl orange is used.
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